On raw milk - 2024

Proficiency testing

Home Proficiency testing Physico-chemistry - On raw milk - 2024

Introduction

The proficiency testings and criteria marked with an are covered by the « accréditation n° 1-2473, comparaisons interlaboratoires, portée disponible sur www.cofrac.fr »/« n° 1-2473 accreditation, interlaboratory comparisons, scope available on www.cofrac.fr », and detailed flexible scope available there


Methods / Analytes

fat determined using the Gerber method: 10 samples with fat varying from 15 to 49 g/l

- fat determined using the Röse-Gottlieb method: 10 samples with fat varying from 14.5 to 48g/kg

true protein determined using the Amido Black method: 10 samples with protein varying from 24 to 37g/l

- total and non-protein nitrogen determined using the Kjeldahl or any other method:
- Total nitrogen : 10 samples with nitrogen varying from 3.5 to 6.5 g N/l
- Non-protein nitrogen: 3 samples of milk (NPN about 0.2 to 0.3 g N/l)
- 1 tryptophan solution
- 1 glycine solution in which the nitrogen concentration is equivalent to that of milk
- 1 tryptophan solution
- 1 ammonium sulphate solution
The nitrogen concentration of the solutions is equivalent to that of milk

non-casein nitrogen determined using the Kjeldahl or any other method: 5 samples with casein varying from 0.7 to 1.2 g N/l

- lactose determined using the enzymatic method (or any other method): 10 samples with lactose varying from 4.6 to 5.1 % + 1 lactose solution at a concentration equivalent to that of milk

freezing point determined using the cryoscopic method: 10 samples with freezing point varying from -0.550 to -0.480 °C + 2 standard NaCl solutions for calibration

dry matter (any method): 10 samples with dry matter varying from 10 to 15 %

urea (any method except infrared): 10 samples with urea varying from 100 to 700 mg/l

somatic cells for all methods used: 10 samples containing between 50 000 and 1 600 000 cells/ml + 1 control sample


Number of samples

-1 set of 10 samples which are the same for the Gerber and Amido Black methods
-1 set of 10 samples which are the same for the Kjeldahl and Röse-Gottlieb methods
-1 set of 5 samples specific to the determination of casein
-1 set of 10 samples which are the same for the determination of dry matter and lactose, as well as cryoscopic measurements.
-1 set of 10 samples specific to the determination of urea
-1 set of 10 samples specific to the determination of somatic cells + 1 control sample


Packaging

in 30 ml screw-capped vials with airtight seals


Preservation

addition of Bronopol to the samples (final concentration: 0.02 %)


Dispatch

in insulated box with ice packs by express carrier (see regulation for shipping times)


Storage in the laboratory

at 4 (± 2) °C


Validity of the samples

testing must be carried out within 7 days after the date of dispatch


Calendar of dispatch :

 

Sample dispatch 2024/03/04 2024/06/03 2024/09/02 2024/12/02
Return of results to ACTALIA Cecalait 2024/03/18 2024/06/17 2024/09/16 2024/12/16

Subscription at least 10 days before each dispatch

Rates

Members Non-members
Registration fees per shipment 68.13 € 101.82 €
Participation fee per tested method 68.13 € 101.82 €
Total nitrogen + NPN (Supplement) 13.48 € 20.22 €


Special conditions :

  • For groups from 10 to 24 participating laboratories: 10 % discount,
  • For groups from 25 participating laboratories: 15 % discount

Payment conditions :

within 1 month of receiving invoice

Formulas

  • Fat by Gerber
  • True protein by Amido black
  • Fat by Röse-Gottlieb
  • Total nitrogen + NPN
  • Non-casein nitrogen
  • Dry matter
  • Lactose
  • Freezing point by cryoscopy
  • Urea
  • Somatic cells




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ACTALIA Cecalait

Rue de Versailles
BP 70129
39801 POLIGNY CEDEX
FRANCE

Tel : +33 (0)3 84 73 63 20
Fax : +33 (0)3 84 73 63 29

cecalait[at]actalia.eu

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